Mixing Ferric Ammonium Oxalate
I bought some AFO to try Mike Ware's POP palladium method, and have a
question about mixing it.
From Ware's site:
Within 5 minutes nearly all the solid will have dissolved to form an
emerald-green solution. The volume will be correct (50 cc) so it does not
need to be made up. A little remaining solid may be ignored.
Filter the solution (Whatman # 1 paper, is adequate) directly into the
clean, dry, brown storage bottle, and store at room temperature in the
dark.
My question: how much is "a little remaining solid"?
I mixed a 45% solution (Ware's directions call for 60%), and it's still
somewhat milky. I let it sit overnight, and there was still quite a bit
of solid that had settled...about 1/8-1/4 inch in about 2 inches of
chemistry...60mL bottle.
Also, he says to use a Whatman # 1 paper...is a coffee filter adequate?
Camden Hardy
camden[at]hardyphotography[dot]net
http://www.hardyphotography.net