RE: Sodium chloropalladite and Ziatype, now on to making AFO

From: Baird, Darryl ^lt;dbaird@umflint.edu>
Date: 01/18/04-02:41:00 PM Z
Message-id: <37885B2630DF0C4CA95EFB47B30985FB04525C83@Exchange-1.umflint.edu>

Has anyone made their own ammonium ferric oxalate (AFO) from ammonium
carbonate and oxalic acid? What was your experience?

The "formulary" at B&S states to make AFO, simply nuetralize oxalic
acid with either ammonium or ammonium carbonate. I had the later and
mixed equal parts (by weight) together into about 100ml of distilled
water. After the fizzy stuff stopped, I vigorously stirred the
concoction and then poured through a coffee filter, allowed to strain,
and then spread the resulting white paste onto a glass sheet to dry.
Is this an appropriate way to "nuetralize" or I'm likely to have
missed a step or messed up the desired AFO?

thanks

Darryl

Received on Sun Jan 18 14:47:18 2004

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