From: Sandy King (sanking@hubcap.clemson.edu)
Date: 12/24/00-12:33:34 PM Z
Joe,
Now that I have seen how viable the kallitype process is for me, both 
for its own qualities and for the fact that it is perfectly balanced 
in speed to carbon printing, I have gone back and looked at some of 
the things that need to be done to maximize the stability of the 
process. What I have decided to do is use two separate  clearing 
baths after development, one of EDTA, the other of Citric Acid, each 
for two minutes. I will also use a 1.5% sodium sulfite solution after 
fixing to eliminate the hypo problem.
I made another kallitype today, this one toned with a 1:100 Rapid 
Sodium Sulfite solution. There was no bleaching of the image at all 
with this toner, either during toning or afterward in the fixer. The 
platinum toner lead to a slight loss of density, as I noted in my 
previous message. Any thoughts on what gold might do?
Sandy
>Sandy,
>
>Congratulations on your first kallitype.  Nice process, isn't it? I would
>like to make one suggestion.  In the future, add a clearing step after the
>developer.  Like platinum or palladium printing the excess ferrous compounds
>need to be removed. Rinse the developed print for one minute in running
>water. Clear the print for a couple minutes in a bath of citric acid or EDTA
>with constant agitation.  The recipe for the clearing bath is a couple of
>tablespoons full of either citric acid or EDTA in a liter of water at room
>temperture. Then follow by a minute rinse in running water. Tone and fix as
>usual.
>
>Joe
>
>
>
>----- Original Message -----
>From: Sandy King <sanking@hubcap.clemson.edu>
>To: <alt-photo-process-l@sask.usask.ca>
>Cc: <stwang@clemson.edu>
>Sent: Saturday, December 23, 2000 6:57 PM
>Subject: First kallitype
>
>
>>  Well, beginners luck or what I made an absolutely first rate
>>  kallitype from one of my 7X17 negatives on the very first try. I did
>>  not even make a test print, just exposed the negative exactly as I
>>  had for making a carbon. To say that I was stunned by the result, and
>>  by characteristics of the process, is much an understatement. For
>>  anyone interested here is what I did.
>>
>>  1. Coated with a rod a sheet of Bristol Rising 2-ply with the
>>  standard sensitizer described in Farber, using 3ml for the 7X17
>>  negative. I added one drop of 20% Tween to the sensitizer.
>>  2. Left coated paper to air dry for 30 minutes.
>>  3. Exposed with a UV light (BL tubes), with some dodging and burning,
>>  for a time previously established time with this negative for a
>>  carbon print.  DR of negative about 1.6.
>>  4. Developed for 2.0 minutes at room temperature using the sodium
>>  acetate + Tartaric acid developer for neutral gray-black tones. At
>>  this point print was slightly on the heavy side, a little more dense
>>  than previous carbons.
>>  5. Washed print in running water for 5.0 minutes.
>>  6. Toned with platinum (5g of sodium citrate + 5ml of platinum
>>  solution #3 per liter of water) for one minute. The image lost about
>>  1/2 step of density during toning.
>>  7. Washed print for 1.0 minutes in running water.
>>  8. Fixed print for 5.0 minutes in a 2.5% sodium thiosulfate solution.
>>  The print lost no more density during fixing.
>>  9. Washed print for 2.0 minutes in running water.
>>  10. Cleared print for 2.0 minutes in a 3% EDTA solution.
>>  11. Washed print for 10 minutes.
>>  12. Dryed.
>>
>>  Result: Density of print close to perfect. Good deep rich shadows.
>>  Neutral gray/black color.
>>
>>  Thanks to all on the list who offered advice. As one will note  the
>>  working procedures described above combine recommendations from
>>  several published sources but are not identical to any one of them.
>>
>>  Sandy King
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